|本期目录/Table of Contents|

[1]陈云博,刘 欢,张赵灵,等.含氨基硅溶胶的制备及其对真丝织物的阻燃整理[J].丝绸,2018,55(3):031101.[doi:10.3969/j.issn.1001-7003.2018.03.001]
 CHEN Yunbo,LIU Huan,ZHANG Zhaoling,et al.Preparation of amino silica sol and flame retardant finishing of silk fabric[J].Journal of Silk,2018,55(3):031101.[doi:10.3969/j.issn.1001-7003.2018.03.001]
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含氨基硅溶胶的制备及其对真丝织物的阻燃整理(PDF)
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《丝绸》[ISSN:1001-7003/CN:33-1122/TS]

卷:
55
期数:
2018年3期
页码:
031101
栏目:
研究与技术
出版日期:
2018-03-20

文章信息/Info

Title:
Preparation of amino silica sol and flame retardant finishing of silk fabric
文章编号:
1001-7003(2018)03-0001-06
作者:
陈云博刘 欢张赵灵邢铁玲陈国强谈金麒程安康
1.苏州大学 纺织与服装工程学院,江苏 苏州 215021;2.江苏华佳控股集团有限公司,江苏 苏州215200
Author(s):
CHEN Yunbo LIU Huan ZHANG Zhaoling XING Tieling CHEN Guoqiang TAN Jinqi CHENG Ankang
 1.College of Textile & Clothing Engineering, Soochow University, Suzhou, 215021, China; 2. Huajia Group, Suzhou, 215200, China
关键词:
溶胶-凝胶氨基硅烷苯膦酸阻燃整理真丝织物
Keywords:
sol-gel amino silane phenylphosphonic acid flame retardant finishing silk fabric
分类号:
TS195.2;TQ610.48
doi:
10.3969/j.issn.1001-7003.2018.03.001
文献标志码:
A
摘要:
通过对溶胶-凝胶技术制备出的含氨基硅溶胶与苯膦酸结合,共同整理到真丝织物上,得到具有阻燃性能的真丝织物。讨论溶胶制备工艺和苯膦酸用量对整理后织物阻燃性能的影响,并通过极限氧指数(LOI)、垂直燃烧、烟密度、扫描电镜(SEM)等测试,来表征整理前后真丝织物的结构和性能。结果表明:硅溶胶的制备与N-(3-三甲氧基硅丙基)乙二胺(AEPTES)、C2H5OH、H2O和NaCl的比例,以及溶液的pH值有关;当苯膦酸摩尔质量是0.6 mol/L时,所得到的真丝织物阻燃性能良好,其极限氧指数为29.8%,烟密度为16.98。
Abstract:
Silicon sol containing amino was prepared by sol-gel technology, and was combined with phenylphosphonic acid to finish silk fabric so as to gain the silk fabric with flame retardant property. The influence of silicon sol preparation process and dosage of phenyl phosphonic acid on the flame retardant properties of silk fabrics was discussed. The structure and properties of silk fabrics before and after finishing w tested and characterized by limit oxygen index (LOI), vertical combustion, smoke density, and scanning electron microscopy (SEM). The results show that the preparation process of silica sol (molar ratio) is related to the rate of C2H5OH, H2O, NaCl and (3-(Trimethoxysilyl) propyl) ethane-1,2-diamine (AEPTES), and the pH of solution; when the phenyl phosphonic acid agent is 0.6 mol/L, the silk fabric with good flame retardant properties can be obtained. The limit oxygen index of silk fabric is 29.8% and the smoke density is 16.98

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备注/Memo

备注/Memo:
基金项目:江苏省“青蓝工程”资助项目(苏教师〔2014〕23号);江苏高校优势学科建设工程二期项目(苏学科办〔2014〕9号);江苏省博士后科研基金资助项目(1601025B)
收稿日期:2017-07-17
修回日期:2017-00-00
作者简介:陈云博(1991—),男,硕士研究生,研究方向为功能性纺织品的研发
通信作者:邢铁玲,教授,xingtieling@suda.edu.cn
更新日期/Last Update: 2018-01-15