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[1]郝 旭,崔一帆,路艳华,等.柞丝绸X型活性染料循环染色工艺研究[J].丝绸,2018,55(11):111102.[doi:10.3969/j.issn.1001-7003.2018.11.002]
 HAO Xu,CUI Yifan,LU Yanhua,et al.Study on the recycle dyeing technology of tussah silk fabric dyed with X type reactive dye[J].Journal of Silk,2018,55(11):111102.[doi:10.3969/j.issn.1001-7003.2018.11.002]
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柞丝绸X型活性染料循环染色工艺研究(PDF)
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《丝绸》[ISSN:1001-7003/CN:33-1122/TS]

卷:
55
期数:
2018年11期
页码:
111102
栏目:
研究与技术
出版日期:
2018-11-20

文章信息/Info

Title:
Study on the recycle dyeing technology of tussah silk fabric dyed with X type reactive dye
文章编号:
1001-7003(2018)11-0005-06
作者:
郝 旭崔一帆路艳华李 佳王勃翔程德红
1.辽东学院 辽宁省功能纺织材料重点实验室, 辽宁 丹东118003;2.辽东学院 化学工程学院,辽宁 丹东118003, 3.大连工业大学 纺织与材料工程学院, 辽宁 大连116034
Author(s):
HAO Xu CUI Yifan LU Yanhua LI Jia WANG BoxiangCHENG Dehong
 1.Liaoning Province Key Laboratory of Functional Textile Materials, Eastern Liaoning University, Dandong, 118003, China; 2.College of Chemical Engineering, Eastern Liaoning University Dandong, 118003, China; 3.College of Textile and Material Engineering, Dalian Polytechnic University, Dalian,116034, China
关键词:
柞丝绸X型活性染料染料激活循环染色废水减排
Keywords:
tussah silk X-type reactive dyes dye activation cycle dyeing wastewater discharge reduction
分类号:
TS193.5
doi:
10.3969/j.issn.1001-7003.2018.11.002
文献标志码:
A
摘要:
为了节约染料和减少染色废水向环境的排放,对活性染料的循环染色进行了研究。首先对染色残液中的水解活性染料通过中和法再生,然后利用再生活性染料和补加原染料方法对柞丝绸进行一浴两步法循环染色。采用傅利叶红外光谱对激活前后活性红X-3B染料的结构进行了表征,采用测色配色法对多次循环染色试样进行了测试。结果表明,激活后活性红X-3B染料分别在685 cm-1和621cm-1处具有与原染料一样的氯原子活性基特征峰,激活前后染色试样的K/S值同色性较好,且具有良好的色光和皂洗色牢度,试样的摩擦色牢度和强力指标没有下降,染色残液可以实现24次连续染色。
Abstract:
To save dye s and reduce the discharge of dyeing wastewater to our environment, the recycle dyeing method of reactive dye was studied in this paper. The hydrolyzed reactive red dye X-3B in the dyeing residual liquid was first activated with neutralization method, and then the regenerated reactive dye was used to dye tussah silk fabric with the method of one-bath two-step by adding the original dye. FT-IR spectra were used to characterize the structures of the dye before and after activation, and the method of color measurement and matching was used to test the dyed tussah samples. The results indicated that the activated reactive red X - 3 B dye showed the characteristic peaks of helium atom active group at 685 cm -1 and 621 cm -1 like the original dye. On the other hand, K/S values of the dyed tussah samples before and after activation had the good consistency, and color right and washing fastness were good. the values of rubbing fastness and strength index did not?decline. The residual liquid can achieve continuous coloring for 24 times.

参考文献/References:

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备注/Memo

备注/Memo:
基金项目:辽宁省自然科学基金资助项目(2016341)
收稿日期:2018-02-06
修回日期:2018-00-00
作者简介:郝旭(1964—),男,高级实验师,主要从事纤维材料的功能化和生态染整技术的研究
更新日期/Last Update: 2018-10-15