|本期目录/Table of Contents|

[1]李邦玉.水溶性聚合物整理丝绸研究[J].丝绸,2019,56(3):031103.
 LI Bangyu.Study on water soluble polymer in silk finishing[J].Journal of Silk,2019,56(3):031103.
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水溶性聚合物整理丝绸研究(PDF)
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《丝绸》[ISSN:1001-7003/CN:33-1122/TS]

卷:
56
期数:
2019年3期
页码:
031103
栏目:
研究与技术
出版日期:
2019-03-20

文章信息/Info

Title:
Study on water soluble polymer in silk finishing
文章编号:
1001-7003(2019)00-0000-00
作者:
李邦玉
苏州市职业大学 应用化学研究室, 江苏 苏州 215104
Author(s):
LI Bangyu
Institute of Applied Chemistry, Suzhou Vocational University, Suzhou 215104, China
关键词:
水溶性聚合物丝绸微波整理性能表征抗起毛
Keywords:
water soluble polymer silk microwave finishing property characterization anti-pilling
分类号:
TS195.644
doi:
-
文献标志码:
A
摘要:
提高丝绸抗起毛能力是提升绣品质量的重要保障之一。用2%水溶性聚合物A浸润丝绸单丝束,合适功率的微波加热交联固化。整理过的丝绸单丝束样品经过红外光谱及X射线粉末衍射表征、扫描电镜和光学显微镜观察。实验结果显示,350 W微波功率加热4 min过的单丝束的聚集度大幅度提高,样品的色度没有明显下降、丝绸手感比较柔软,拉伸强度略有增强,耐摩擦能力明显提高。在此基础上,进一步优化工艺条件,可以为刺绣等产品的防起毛整理产业化提供技术支持。
Abstract:
Improving the anti-pilling ability of silk is one of the important guarantees for improving the quality of embroidery. The silk monofilament was impregnated with 2% water soluble polymer A , cross-linked and solidified by microwave heating at a suitable power. The finished silk samples were characterized by infrared spectroscopy, X-ray powder diffraction, scanning electron microscopy and optical microscopy. The experimental results showed that the concentration of the monofilament bundle heated by 350 W microwave power for 4 min greatly improved . The chroma of the sample did not significantly decrease. The silk was soft. The tensile strength was slightly enhanced, and the friction resistance obviously improved. On this basis, further optimization of the process conditions may provide technical support for the anti-pilling finishing industrialization of products such as embroidery.

参考文献/References:

[1]黄阳阳, 夏云, 顾伟. 聚丙烯酸对刺绣防起毛处理研究[J]. 江苏丝绸, 2016(6): 19-22.
HUANG Yangyang, XIA Yun, GU Wei. Polyacrylic acid on the anti-pilling treatment of embroidery [J] Jiangsu silk, 2016 (6): 19-22.
[2]雷春堂, 潘晓勇, 姚国红, 等. 水溶性聚乙烯醇的研究进展[J]. 塑料工业, 2011, 39(2): 10-13.
LEI Chuntang,PAN Xiaoyong, YAO Guohong, et al. Progress in water-soluble polyvinyl alcohol [J]. China Plastics Industry, 2011, 39(2): 10-13.
[3]PANAITESCU D M, FRONE A N, GHIUREA M, et al. Influence of storage conditions on starch/PVA films containing cellulose nanofibers [J]. Industrial Crops and Products, 2015, 70: 170-177.
[4]孙义明, 周建刚, 彭少贤, 等. 薄膜用聚乙烯醇改性的研究现状及进展[J]. 包装工程, 2004, 25(3): 4-6.
SUN Yiming, ZHOU Jiangang, PENG Shaoxian, et al. The recent situation and progress of study on PVA used for films[J]. Packaging Engineering, 2004, 25(3): 4-6.
[5]施茹玲, 周文富. 无毒高相对分子质量PVA的合成与结构分析研究[J]. 应用化工, 2008, 37(4): 391-395.
SHI Ruling, ZHOU Wenfu. Synthesis and structure analysis of nontoxic high molecular weight of PVA [J]. Applied Chemical Industry, 2008, 37(4): 391-395.
[6]李阳博, 吴文倩, 刘哲伟, 等. PVA 复合薄膜水果保鲜研究[J]. 中国塑料, 2010,24(4): 80-85.
LI Yangbo, WU Wenqian, LIU Zhewei, et al. Study on fresh-keeping poly(vinyl alcohol)composite films for fruits [J]. China Plastics, 2010,24(4): 80-85.
[7]施媚梧.微波辐照下丝绸接枝丙三醇缩水甘油醚[J]. 丝绸, 1998(8): 25-28.
SHI Meiwu. Silk-grafted glycerol shrinking sun oil ether under microwave irradiation [J]. Journal of Silk , 1998(8): 25-28.
[8]高红艳, 许强, 杨志怀. FT-IR 在研究蛋白质二级结构中的应用[J]. 宝鸡文理学院学报(自然科学版), 2009(3): 47-53.
GAO Hongyan , XU Qiang ,YANG Zhihuai. Research on protein secondary structure by Fourier transformation infrared spectroscopy [J]. Journal of Baoji University of Arts and Sciences (Natural Science Edition ), 2009(3): 47-53.
[9]陈国强.甲基丙烯酸羟丙醋接枝交联真丝绸结构与性能的研究[J]. 浙江丝绸工学院学报, 1998, 15(4): 277-281.
CHEN Guoqiang. Studies on prope rties of the silk fabric grafted (cross-linked) with hydroxypropyl methacrylate [J]. Journal of Zhejiang Institute of Silk Textiles, 1998,15(4): 277-281.
[10]冉瑞龙, 龙家杰, 徐水, 等. 超临界CO2 流体处理对蚕丝纤维结构的影响[J]. 丝绸, 2006(5): 22-24.
RAN Ruilong, LONG Jiajie, XU Shui, et al. Effect of supercritical CO2 treatment on the structure of silk [J]. Journal of Silk, 2006(5): 22-24 .
[11]NAYAK R R, SUKLA L B, MISHRA B K. Low temperature oxygen plasma assisted surface modification of raw silk fibre and their characterizations [J]. International Journal of Plastics Technology, 2013, 17(1): 1-9.
[12]周颖, 许建梅. 生丝单丝强度、伸长率与拉伸速度相关性分析[J]. 丝绸, 2010(6): 8-10.
ZHOU Ying, XU Jianmei. Relevent analysis on single-silk intensity, elongation and drawing speed of raw silk [J]. Journal of Silk, 2010(6): 8-10.
[13]邹利云, 陈宇岳, 盛家镛, 等. 微波辐照后的真丝纤维结构及其性能研究[J] 丝绸, 2001(4): 20-22.
ZOU Liyun, CHEN Yuyue, SHENG Jiayong, et al . Study on the structure and properties of silk fibers treated by microwave [J]. Journal of Silk, 2001(4): 20-22.
[14]施楣梧, 马步虎. 微波辐照下丝绸内部结构和力学性能的变化[J]. 苏州丝绸工学院学报, 1996, 16(3): 22-26.

备注/Memo

备注/Memo:
基金项目: 苏州市科学技术局民生工程项目(SS201742)
收稿日期:2018-09-21
修回日期: 2018-00-00
作者简介: 李邦玉(1968—),男,教授,博士, 主要从事化学及材料科学的研究
更新日期/Last Update: 2019-01-18